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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">cvmet</journal-id><journal-title-group><journal-title xml:lang="ru">Известия вузов. Цветная металлургия</journal-title><trans-title-group xml:lang="en"><trans-title>Izvestiya. Non-Ferrous Metallurgy</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">0021-3438</issn><issn pub-type="epub">2412-8783</issn><publisher><publisher-name>НИТУ МИСИС</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.17073/0021-3438-2018-3-36-48</article-id><article-id custom-type="elpub" pub-id-type="custom">cvmet-773</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>Обработка металлов давлением</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>Pressure Treatment of Metals</subject></subj-group></article-categories><title-group><article-title>ЗАКОНОМЕРНОСТИ ФОРМИРОВАНИЯ И ДЕГРАДАЦИИ МИКРОСТРУКТУРЫ И СВОЙСТВ НОВЫХ УЛЬТРАМЕЛКОЗЕРНИСТЫХ НИЗКОМОДУЛЬНЫХ СПЛАВОВ СИСТЕМЫ Ti–Nb–Mo–Zr</article-title><trans-title-group xml:lang="en"><trans-title>REGULARITIES OF FORMATION AND DEGRADATION OF THE MICROSTRUCTURE AND PROPERTIES OF NEW ULTRAFINE-GRAINED LOW-MODULUS Ti–Nb–Mo–Zr ALLOYS</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Колобов</surname><given-names>Ю. Р.</given-names></name><name name-style="western" xml:lang="en"><surname>Kolobov</surname><given-names>Yu. R.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Доктор физико математических наук, профессор, зав. кафедрой наноматериалов и нанотехнологий НИУ БелГУ на базе Научного центра РАН в Черноголовке; зав. лабораторией физико-химической инженерии композиционных материалов ИПХФ РАН </p><p>308034, г. Белгород, ул. Королева, 2а</p></bio><bio xml:lang="en"><p>Dr. Sci. (Phys.-Math.), prof., head of the Department of the nanomaterials and nanotechnologies of the Belgorod State National Research University on the basis of the Scientific Center of RAS in Chernogolovka; head of the Laboratory of the physico-chemical engineering of composite materials of the Institute of Problems of Chemical Physics of RAS </p><p>308034, Russia, Belgorod, Korolev str., 2а</p></bio><email xlink:type="simple">kolobov@bsu.edu.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Голосова</surname><given-names>О. А.</given-names></name><name name-style="western" xml:lang="en"><surname>Golosova</surname><given-names>O. A.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Младший научный сотрудник ИСМАН </p><p>142432, Московская обл., г. Черноголовка, ул. Академика Осипьяна, 8</p></bio><bio xml:lang="en"><p>Junior researcher </p><p>142432, Russia, Chernogolovka, Academician Osipyan pr., 8</p></bio><email xlink:type="simple">golosova@ism.ac.ru</email><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Манохин</surname><given-names>С. С.</given-names></name><name name-style="western" xml:lang="en"><surname>Manokhin</surname><given-names>S. S.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Кандидат технических наук, старший научный сотрудник лаборатории физико-химической инженерии композиционных материалов ИПХФ РАН</p><p>142432, Московская обл., г. Черноголовка, пр. Академика Семенова, 1 </p></bio><bio xml:lang="en"><p>Cand. Sci. (Tech.), senior researcher of Laboratory of the physico-chemical engineering of composite materials </p><p>142432, Russia, Chernogolovka, Academician Semenov pr., 1</p></bio><email xlink:type="simple">manohin@bk.ru</email><xref ref-type="aff" rid="aff-3"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>Белгородский государственный национальный исследовательский университет (НИУ БелГУ); &#13;
Институт проблем химической физики (ИПХФ) РАН</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Belgorod State National Research University on the basis of the Scientific Center of RAS in Chernogolovka; &#13;
Institute of Problems of Chemical Physics of RAS</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="ru"><institution>Институт структурной макрокинетики и проблем материаловедения им. А.Г. Мержанова РАН (ИСМАН)</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Merzhanov Institute of Structural Macrokinetics and Materials Science of RAS</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-3"><aff xml:lang="ru"><institution>Институт проблем химической физики (ИПХФ) РАН</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Institute of Problems of Chemical Physics of RAS</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2018</year></pub-date><pub-date pub-type="epub"><day>14</day><month>06</month><year>2018</year></pub-date><volume>0</volume><issue>3</issue><fpage>36</fpage><lpage>48</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Колобов Ю.Р., Голосова О.А., Манохин С.С., 2018</copyright-statement><copyright-year>2018</copyright-year><copyright-holder xml:lang="ru">Колобов Ю.Р., Голосова О.А., Манохин С.С.</copyright-holder><copyright-holder xml:lang="en">Kolobov Y.R., Golosova O.A., Manokhin S.S.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://cvmet.misis.ru/jour/article/view/773">https://cvmet.misis.ru/jour/article/view/773</self-uri><abstract><p>Исследованы закономерности формирования ультрамелкозернистой (УМЗ) и субмикрокристаллической (СМК) структур в новых безникелевых низкомодульных титановых β-сплавах системы Ti–Nb–Mo–Zr в условиях воздействия пластической деформации. Определены температурно-временные интервалы развития процессов динамической рекристаллизации при одновременном влиянии температуры и пластической деформации. На примере сплава Ti–28Nb–8Mo–12Zr построена и проанализирована диаграмма рекристаллизации второго рода. В изучаемых титановых сплавах с использованием растровой электронной микроскопии и метода дифракции обратно-рассеянных электронов установлена возможность получения УМЗ-структуры с размером зерен не более 7 мкм при высокой доле большеугловых границ зерен. Показано, что формирование УМЗ-структуры приводит к заметному увеличению прочностных и пластических характеристик исследуемых сплавов. Изучены закономерности формирования УМЗи СМК-структур при воздействии пластической деформации в сплаве Ti–28Nb–8Mo–12Zr (метод продольной прокатки) и в промышленном β-сплаве ВТ30 (метод поперечно-винтовой прокатки). Поперечно-винтовая прокатка позволяет получить однородное УМЗ-состояние в сплаве ВТ30, в отличие от разработанного β-сплава Ti–28Nb–8Mo–12Zr, в котором данный метод приводит к разуплотнению структуры в центральной области с образованием микропор и микротрещин. Для этого сплава удается сформировать наноструктурированное состояние со средним размером зерен порядка 100 нм при использовании обработки методом кручения под высоким давлением.</p></abstract><trans-abstract xml:lang="en"><p>Regularities of the formation of ultrafine-grained (UFG) and submicrocrystalline (SMC) structures in new nickel-free low-modulus Ti–Nb–Mo–Zr titanium β alloys under the action of plastic deformation were studied. Temperature-time ranges of the development of dynamic recrystallization processes under the simultaneous action of temperature and plastic deformation were determined. The recrystallization diagram of II type of the Ti–28Nb–8Mo–12Zr alloy was constructed and analyzed. It was shown using scanning electron microscopy and electron backscatter diffraction method that the UFG structure with an average grain size of no more than 7 μm and high fraction of high-angle grain boundaries is formed in the investigated alloys as a result of longitudinal rolling followed by annealing for quenching. It was found that the formation of the UFG structure leads to a significant increase in the strength and plastic characteristics of these alloys. The regularities of the formation of UFG and SMC structures in the titanium β alloys Ti–28Nb–8Mo–12Zr and VT30 widely used in industry under the action of plastic deformation by the helical rolling method were studied. It was shown that the helical rolling of the VT30 alloy leads to the formation of the homogeneous UFG state as opposite to the developed Ti–28Nb–8Mo–12Zr β alloy where this method causes structure softening with micropores and microcracks formed in the central region. It is possible to form a nanostructured state with an average grain size of about 100 nm in Ti–Nb–Mo–Zr titanium β alloys using high-pressure torsion method.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>низкомодульный титановый сплав</kwd><kwd>ультрамелкозернистая структура</kwd><kwd>наноструктурированное состояние</kwd><kwd>механические свойства</kwd><kwd>поперечно-винтовая прокатка</kwd><kwd>интенсивная пластическая деформация</kwd></kwd-group><kwd-group xml:lang="en"><kwd>low-modulus titanium alloy</kwd><kwd>ultrafine-grained structure</kwd><kwd>nanostructured state</kwd><kwd>mechanical properties</kwd><kwd>helical rolling</kwd><kwd>severe plastic deformation</kwd></kwd-group><funding-group><funding-statement xml:lang="ru">РАН (№ 0089-2015-0222) и ИСМАН (№ 45.2)</funding-statement></funding-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Колобов Ю.Р. Технологии формирования структуры и свойств титановых сплавов для медицинских имплантатов с биоактивными покрытиями // Российские нанотехнологии. 2009. No. 11—12. С. 69—81.</mixed-citation><mixed-citation xml:lang="en">Kolobov Yu.R. Nanotechnologies for the formation of medical implants based on titanium alloys with bioactive coatings. Nanotechnol. Russ. 2009. Vol. 4. No. 11—12. P. 758—775.</mixed-citation></citation-alternatives></ref><ref id="cit2"><label>2</label><citation-alternatives><mixed-citation xml:lang="ru">Stráskýa J., Harcubaa P., Václavováa K., Horváth K., Landa M., Srba O., Janeček M. Increasing strength of a biomedical Ti—Nb—Ta—Zr alloy by alloying with Fe, Si and O // J. Mechan. Behav. Biomed. Mater. 2017. Vol. 71. P. 329—336.</mixed-citation><mixed-citation xml:lang="en">Stráskýa J., Harcubaa P., Václavováa K., Horváth K., Landa M., Srba O., Janeček M. Increasing strength of a biomedical Ti—Nb—Ta—Zr alloy by alloying with Fe, Si and O. J. Mechan. Behav. Biomed. Mater. 2017. Vol. 71. P. 329—336.</mixed-citation></citation-alternatives></ref><ref id="cit3"><label>3</label><citation-alternatives><mixed-citation xml:lang="ru">Wong J.Y., Bronzino J.D. Biomaterials. Boca Raton: CRC Pres, Taylor &amp; Francis Group, 2007.</mixed-citation><mixed-citation xml:lang="en">Wong J.Y., Bronzino J.D. Biomaterials. Boca Raton: CRC Pres, Taylor &amp; Francis Group, 2007.</mixed-citation></citation-alternatives></ref><ref id="cit4"><label>4</label><citation-alternatives><mixed-citation xml:lang="ru">Gunawarman B., Niinomi M., Akahori T., Souma T., Ikeda M., Tada H. Mechanical properties and microstructure of low cost β-titanium alloys for healthcare applications // Mater. Sci. Eng. C. 2005. Vol. 25. No. 3. P. 304—311.</mixed-citation><mixed-citation xml:lang="en">Gunawarman B., Niinomi M., Akahori T., Souma T., Ikeda M., Tada H. Mechanical properties and microstructure of low cost β-titanium alloys for healthcare applications. Mater. Sci. Eng. C. 2005. Vol. 25. No. 3. P. 304—311.</mixed-citation></citation-alternatives></ref><ref id="cit5"><label>5</label><citation-alternatives><mixed-citation xml:lang="ru">Geetha M., Singh A.K., Asokamani R., Gogia A.K. Ti based biomaterials, the ultimate choice for orthopedic implants: A review // Progr. Mater. Sci. 2009. Vol. 54. P. 397—425.</mixed-citation><mixed-citation xml:lang="en">Geetha M., Singh A.K., Asokamani R., Gogia A.K. Ti based biomaterials, the ultimate choice for orthopedic implants: A review. Progr. Mater. Sci. 2009. Vol. 54. P. 397—425.</mixed-citation></citation-alternatives></ref><ref id="cit6"><label>6</label><citation-alternatives><mixed-citation xml:lang="ru">Yaszemski M.J., Trantolo D.J., Lewandrowski K., Hasirci V. Biomaterials in orthopedics. N.Y.: Marcel Dekker, 2004.</mixed-citation><mixed-citation xml:lang="en">Yaszemski M.J., Trantolo D.J., Lewandrowski K., Hasirci V. Biomaterials in orthopedics. N.Y.: Marcel Dekker, 2004.</mixed-citation></citation-alternatives></ref><ref id="cit7"><label>7</label><citation-alternatives><mixed-citation xml:lang="ru">Long Marc, Rack H.J. Titanium alloys in total joint replacement — a material science perspective // Biomaterials. 1998. Vol. 19. P. 1621—1639.</mixed-citation><mixed-citation xml:lang="en">Long Marc, Rack H.J. Titanium alloys in total joint replacement — a material science perspective. Biomaterials. 1998. Vol. 19. P. 1621—1639.</mixed-citation></citation-alternatives></ref><ref id="cit8"><label>8</label><citation-alternatives><mixed-citation xml:lang="ru">Эппле M. Биоматериалы и биоминерализация / Пер. с нем. под ред. В.Ф. Пичугина, Ю.П. Шаркеева, И.А. Хлусова. Томск: Ветер, 2007.</mixed-citation><mixed-citation xml:lang="en">Epple M. Biomaterialien und biomineralisation. Wiesbaden: Vieweg + Teubner Verlag, 2003.</mixed-citation></citation-alternatives></ref><ref id="cit9"><label>9</label><citation-alternatives><mixed-citation xml:lang="ru">Peterson D.R., Bronzino J.D. Biomechanics principles and applications. Boca Raton: CRC Pres, Taylor &amp; Francis Group, 2008.</mixed-citation><mixed-citation xml:lang="en">Peterson D.R., Bronzino J.D. Biomechanics principles and applications. Boca Raton: CRC Pres, Taylor &amp; Francis Group, 2008.</mixed-citation></citation-alternatives></ref><ref id="cit10"><label>10</label><citation-alternatives><mixed-citation xml:lang="ru">Niinomi M., Nakai M., Heida J. Development of new metallic alloys for biomedical applications // Acta Biomater. 2012. Vol. 8. I. 11. P. 3888—3903.</mixed-citation><mixed-citation xml:lang="en">Niinomi M., Nakai M., Heida J. Development of new metallic alloys for biomedical applications. Acta Biomater. 2012. Vol. 8. I. 11. P. 3888—3903.</mixed-citation></citation-alternatives></ref><ref id="cit11"><label>11</label><citation-alternatives><mixed-citation xml:lang="ru">Leyens C., Peter M. Titanium and titanium alloys: Fundamentals and applications. Weinheim: Wiley-VCH, 2003.</mixed-citation><mixed-citation xml:lang="en">Leyens C., Peter M. Titanium and titanium alloys. Fundamentals and applications. Weinheim: Wiley-VCH, 2003.</mixed-citation></citation-alternatives></ref><ref id="cit12"><label>12</label><citation-alternatives><mixed-citation xml:lang="ru">Ranter B.D., Hoffman A.S., Schoen F.J., Lemons J.E. Biomaterials science: An introduction to materials in medicine. 2-nd ed. San Diego: Elsevier Academic Press, 2004.</mixed-citation><mixed-citation xml:lang="en">Ranter B.D., Hoffman A.S., Schoen F.J., Lemons J.E. Biomaterials Science: An introduction to materials in medicine. 2-nd ed. San Diego: Elsevier Academic Press, 2004.</mixed-citation></citation-alternatives></ref><ref id="cit13"><label>13</label><citation-alternatives><mixed-citation xml:lang="ru">Hanawa T., Hiromoto S., Yamamoto A. Metallic biomaterials in body fluid and their surface modification // Structural biomaterials for the 21 century. New Orleans: TMS, 2001. P. 145—154.</mixed-citation><mixed-citation xml:lang="en">Hanawa T., Hiromoto S., Yamamoto A. Metallic biomaterials in body fluid and their surface modification. In: Structural biomaterials for the 21 century. New Orleans: TMS, 2001. P. 145—154.</mixed-citation></citation-alternatives></ref><ref id="cit14"><label>14</label><citation-alternatives><mixed-citation xml:lang="ru">Niinomi M. Recent research and development in titanium alloys for biomedical applications and healthcare goods // Sci. Technol. Adv. Mater. 2003. Vol. 4. P. 445—454.</mixed-citation><mixed-citation xml:lang="en">Niinomi M. Recent research and development in titanium alloys for biomedical applications and healthcare goods. Sci. Technol. Adv. Mater. 2003. Vol. 4. P. 445—454.</mixed-citation></citation-alternatives></ref><ref id="cit15"><label>15</label><citation-alternatives><mixed-citation xml:lang="ru">Lee C.M., C.P. Ju, Lin J.H. Chern. Structure-property relationship of cast Ti—Nb alloys // J. Oral Rehabilitation. 2002. Vol. 29. P. 314—322.</mixed-citation><mixed-citation xml:lang="en">Lee C.M., C.P. Ju, Lin J.H. Chern. Structure-property r elationship of cast Ti—Nb alloys. J. Oral Rehabilitation. 2002. Vol. 29. P. 314—322.</mixed-citation></citation-alternatives></ref><ref id="cit16"><label>16</label><citation-alternatives><mixed-citation xml:lang="ru">Коллеров М.Ю., Ильин А.А., Скворцова С.В. Влияние системы и степени легирования на характеристики эффекта запоминания формы титановых сплавов // Металлы. 2001. No. 2. С. 74—78.</mixed-citation><mixed-citation xml:lang="en">Kollerov M.Yu., Il’in A.A., Skvortsova S.V. Vliyanie sistemy i stepeni legirovaniya na kharakteristiki effekta zapominaniya formy titanovykh splavov [Effect of system and degree of alloying on the characteristics of shape memory effect of titanium alloys]. Metally. 2001. No. 2. P. 74—78.</mixed-citation></citation-alternatives></ref><ref id="cit17"><label>17</label><citation-alternatives><mixed-citation xml:lang="ru">Шереметьев В.А., Прокошкин С.Д., Браиловский В., Дубинский С.М., Коротицкий А.В., Филонов С.М., Петржик М.И. Исследование стабильности структуры и сверхупругого поведения термомеханически обработанных сплавов с памятью формы Ti—Nb—Zr и Ti—Nb—Ta // Физика металлов и металловедение. 2015. Т. 116. No. 4. С. 437—448.</mixed-citation><mixed-citation xml:lang="en">Sheremet’ev V.A., Prokoshkin S.D., Brailovskii V., Dubinskii S.M., Korotitskii A.V., Filonov S.M., Petrzhik M.I. Investigation of the structure stability and superelastic behavior of thermomechanically treated Ti—Nb—Zr and Ti— Nb—Ta shape-memory alloys. Phys. Met. Metallogr. 2015. Vol. 116. No. 4. P. 413—422.</mixed-citation></citation-alternatives></ref><ref id="cit18"><label>18</label><citation-alternatives><mixed-citation xml:lang="ru">Конопацкий А.С., Жукова Ю.С., Дубинский С.М., Коробкова А.А., Филонов М.Р., Прокошкин С.Д. Микроструктурa слитков сверхупругих сплавов на основе Ti— Nb медицинского назначения // Металлург. 2016. No. 2. С. 89—93.</mixed-citation><mixed-citation xml:lang="en">Konopatskii A.S., Zhukova Yu.S., Dubinskii S.M., Korobkova A.A., Filonov M.R., Prokoshkin S.D. Microstructure of superplastic alloys based on Ti—Nb for medical purposes. Metallurgist. 2016. Vol. 60. P. 223—228.</mixed-citation></citation-alternatives></ref><ref id="cit19"><label>19</label><citation-alternatives><mixed-citation xml:lang="ru">Niinomi M. Metallic biomaterials // Jaр. Soc. Artif. Org. 2008. Vol. 11. No. 3. P. 105—110.</mixed-citation><mixed-citation xml:lang="en">Niinomi M. Metallic biomaterials. Jap. Soc. Artif. Org. 2008. Vol. 11. No. 3. P. 105—110.</mixed-citation></citation-alternatives></ref><ref id="cit20"><label>20</label><citation-alternatives><mixed-citation xml:lang="ru">Sakaguchi N., Niinomi M., Akahori T., Takeda J., Toda H. Relationships between tensile deformation behavior and microstructure in Ti—Nb—Ta—Zr system alloys // Mater. Sci. Eng. C. 2005. No. 25. P. 363—369.</mixed-citation><mixed-citation xml:lang="en">Sakaguchi N., Niinomi M., Akahori T., Takeda J., Toda H. Relationships between tensile deformation behavior and microstructure in Ti—Nb—Ta—Zr system alloys. Mater. Sci. Eng. C. 2005. No. 25. P. 363—369.</mixed-citation></citation-alternatives></ref><ref id="cit21"><label>21</label><citation-alternatives><mixed-citation xml:lang="ru">Conzalez M., Pena J., Manero J.M., Arciniegas M., Gil F.J. Design and characterization of new Ti—Nb—Hf alloys // J. Mater. Eng. Perform. 2009. Vol. 18 (5–6). P. 490—495.</mixed-citation><mixed-citation xml:lang="en">Conzalez M., Pena J., Manero J.M., Arciniegas M., Gil F.J. Design and characterization of new Ti—Nb—Hf alloys. J. Mater. Eng. Perform. 2009. Vol. 18(5—6). P. 490—495.</mixed-citation></citation-alternatives></ref><ref id="cit22"><label>22</label><citation-alternatives><mixed-citation xml:lang="ru">Nitta K., Watanabe S., Masahashi N. Ni-free Ti—Nb—Sn shape memory alloys // Structural biomaterials for the 21 century. New Orleans: TMS, 2001. P. 25—34.</mixed-citation><mixed-citation xml:lang="en">Nitta K., Watanabe S., Masahashi N. Ni-free Ti—Nb—Sn shape memory alloys. In: Structural biomaterials for the 21 century. New Orleans: TMS, 2001. P. 25—34.</mixed-citation></citation-alternatives></ref><ref id="cit23"><label>23</label><citation-alternatives><mixed-citation xml:lang="ru">Kawashima A., Watanabe S., Asami K., Hanada S. XPS study of corrosion behavior of Ti—18Nb—4Sn shape memory alloy in a 0,05 mass.% HCl solution // Mater. Trans. 2003. Vol. 44. No. 7. P. 1405—1411.</mixed-citation><mixed-citation xml:lang="en">Kawashima A., Watanabe S., Asami K., Hanada S. XPS study of corrosion behavior of Ti—18Nb—4Sn shape memory alloy in a 0,05 mass. % HCl solution. Mater. Trans. 2003. Vol. 44. No. 7. P. 1405—1411.</mixed-citation></citation-alternatives></ref><ref id="cit24"><label>24</label><citation-alternatives><mixed-citation xml:lang="ru">Колобов Ю.Р., Валиев Р.З., Грабовецкая Г.П. Зернограничная диффузия и свойства наноструктурных материалов. Новосибирск: Наука, 2001.</mixed-citation><mixed-citation xml:lang="en">Kolobov Yu.R., Valiev R.Z., Grabovetskaya G.P. Grainboundary diffusion and properties of nanostructured materials. UK: Cambridge Int. Science Publishing, 2007.</mixed-citation></citation-alternatives></ref><ref id="cit25"><label>25</label><citation-alternatives><mixed-citation xml:lang="ru">Колобов Ю.Р., Липницкий А.Г., Иванов М.Б., Голосов Е.В. Роль диффузионно-контролируемых процессов в формировании структуры и свойств металлических наноматериалов // Композиты и наноструктуры. 2009. No. 2. С. 5—24.</mixed-citation><mixed-citation xml:lang="en">Kolobov Yu.R., Lipnitskii A.G., Ivanov M.B., Golosov E.V. Rol’ diffuzionno-kontroliruemykh protsessov v formirovanii struktury i svoistv metallicheskikh nanomaterialov [Role of the diffusion-controlled processes in the formation of structure and properties of metallic materials]. Composity i nanostructury. 2009. No. 2. P. 5—24.</mixed-citation></citation-alternatives></ref><ref id="cit26"><label>26</label><citation-alternatives><mixed-citation xml:lang="ru">Андриевский Р.А., Глезер А.М. Прочность наноструктур // Успехи физ. наук. 2009. Т. 179. No. 4. С. 337— 358.</mixed-citation><mixed-citation xml:lang="en">Andrievskii R.A., Glezer A.M. Prochnost’ nanostruktur [Strength of nanostructures]. Uspekhi fizicheskikh nauk. 2009. Vol. 179. No. 4. P. 337—358.</mixed-citation></citation-alternatives></ref><ref id="cit27"><label>27</label><citation-alternatives><mixed-citation xml:lang="ru">Dubinskiy S., Brailovski V., Prokoshkin S., Pushin V., Inaekyan K., Sheremetyev V., Petrzhik M., Filonov M. Structure and properties of Ti—19,7Nb—5,8Ta shape memory alloy subjected to thermomechanical Processing including aging // J. Mater. Eng. Perform. 2013. Vol. 22. I. 9. P. 2656—2664.</mixed-citation><mixed-citation xml:lang="en">Dubinskiy S., Brailovski V., Prokoshkin S., Pushin V., Inaekyan K., Sheremetyev V., Petrzhik M., Filonov M. Structure and properties of Ti—19,7Nb—5,8Ta shape memory alloy subjected to thermomechanical Processing including aging. J. Mater. Eng. Perform. 2013. Vol. 22. I. 9. P. 2656—2664.</mixed-citation></citation-alternatives></ref><ref id="cit28"><label>28</label><citation-alternatives><mixed-citation xml:lang="ru">Hao Y.L., Zhang Z.B., Li S.J., Yang R. Microstructure and mechanical behavior of a Ti—24Nb—4Zr—8Sn alloy processed by warm swaging and warm rolling // Acta Mater. 2012. Vol. 60. P. 2169—2177.</mixed-citation><mixed-citation xml:lang="en">Hao Y.L., Zhang Z.B., Li S.J., Yang R. Microstructure and mechanical behavior of a Ti—24Nb—4Zr—8Sn alloy processed by warm swaging and warm rolling. Acta Mater. 2012. Vol. 60. P. 2169—2177.</mixed-citation></citation-alternatives></ref><ref id="cit29"><label>29</label><citation-alternatives><mixed-citation xml:lang="ru">Václavováa K., Stráskýa J., Veselý J., Gatina S., Polyakova V., Semenova I., Janeček M. Evolution of microstructure and microhardness in Ti—15Mo β-Ti alloy prepared by high pressure torsion // Mater. Sci. Forum. 2016. Vol. 879. I. 9. P. 2555—2560.</mixed-citation><mixed-citation xml:lang="en">Václavováa K., Stráskýa J., Veselý J., Gatina S., Polyakova V., Semenova I., Janeček M. Evolution of microstructure and microhardness in Ti-15Mo β-Ti alloy prepared by high pressure torsion. Mater. Sci. Forum. 2016. Vol. 879. I. 9. P. 2555—2560.</mixed-citation></citation-alternatives></ref><ref id="cit30"><label>30</label><citation-alternatives><mixed-citation xml:lang="ru">Gatina S., Semenova I., Leuthold J., Valiev R. Nanostructuring and phase transformations in the β-Alloy Ti-15Mo during high-pressure torsion // Adv. Eng. Mater. 2015. Vol. 17. No. 12. P. 1742—1747.</mixed-citation><mixed-citation xml:lang="en">Gatina S., Semenova I., Leuthold J., Valiev R. Nanostructuring and phase transformations in the β-Alloy Ti-15Mo during high-pressure torsion. Adv. Eng. Mater. 2015. Vol. 17. No. 12. P. 1742—1747.</mixed-citation></citation-alternatives></ref><ref id="cit31"><label>31</label><citation-alternatives><mixed-citation xml:lang="ru">Janeček M., Čížek J., Stráskýa J., Václavováa K., Hruška P., Polyakova V., Gatina S., Semenova I. Microstructure evolution in solution treated Ti15Mo alloy processed by high pressure torsion // Mater. Charact. 2014. Vol. 98. P. 233—240.</mixed-citation><mixed-citation xml:lang="en">Janeček M., Čížek J., Stráskýa J., Václavováa K., Hruška P., Polyakova V., Gatina S., Semenova I. Microstructure evolution in solution treated Ti15Mo alloy processed by high pressure torsion. Mater. Charact. 2014. Vol. 98. P. 233—240.</mixed-citation></citation-alternatives></ref><ref id="cit32"><label>32</label><citation-alternatives><mixed-citation xml:lang="ru">Yilmazer H., Niinomi M., Nakai M., Cho K., Hieda J., Todaka Y., Miyazaki T. Mechanical properties of a medical β-type titanium alloy with specific microstructural evolution through high-pressure torsion // Mater. Sci. Eng. C. 2013. Vol. 33. P. 2499—2507.</mixed-citation><mixed-citation xml:lang="en">Yilmazer H., Niinomi M., Nakai M., Cho K., Hieda J., Todaka Y., Miyazaki T. Mechanical properties of a medical β-type titanium alloy with specific microstructural evolution through high-pressure torsion. Mater. Sci. Eng. C. 2013. Vol. 33. P. 2499—2507.</mixed-citation></citation-alternatives></ref><ref id="cit33"><label>33</label><citation-alternatives><mixed-citation xml:lang="ru">Golosova O.A., Ivanov M.B., Vershinina T.N., Kolobov Yu.R. Structure and properties of low modulus titanium alloy Ti—26Nb—7Mo—12Zr // Mater. Sci. Technol. 2013. Vol. 29. No. 2. P. 204—209.</mixed-citation><mixed-citation xml:lang="en">Golosova O.A., Ivanov M.B., Vershinina T.N., Kolobov Yu.R. Structure and properties of low modulus titanium alloy Ti—26Nb—7Mo—12Zr. Mater. Sci. Technol. 2013. Vol. 29. No. 2. P. 204—209.</mixed-citation></citation-alternatives></ref><ref id="cit34"><label>34</label><citation-alternatives><mixed-citation xml:lang="ru">Бетехтин В.И., Колобов Ю.Р., Голосова О.А., Кардашев Б.К., Кадомцев А.Г., Нарыкова М.В., Иванов М.Б., Вершинина Т.Н. Упруго-пластические свойства низкомодульного β-сплава на основе титана // Журн. техн. физики. 2013. Т. 83. Вып. 10. С. 38—43.</mixed-citation><mixed-citation xml:lang="en">Betekhtin V.I., Kolobov Yu.R., Golosova O.A., Kardashev B.K., Kadomtsev A.G., Narykova M.V., Ivanov M.B., Vershinina T.N. Elastoplastic properties of a low-modulus titanium-based β alloy. Technical Phys. 2013. Vol. 58. No. 10. P. 1432—1436.</mixed-citation></citation-alternatives></ref><ref id="cit35"><label>35</label><citation-alternatives><mixed-citation xml:lang="ru">Betekhtin V.I., Kolobov Yu.R., Golosova O.A., Dvorak J., Sklenicka V., Kardashev B.K., Kadomtsev A.G., Narykova M.V., Ivanov M.B. Elastic modulus, microplastic properties and durability of titanium alloys for biomedical applications // Rev. Adv. Mater. Sci. 2016. Vol. 45. No. 1/2. P. 42—51.</mixed-citation><mixed-citation xml:lang="en">Betekhtin V.I., Kolobov Yu.R., Golosova O.A., Dvorak J., Sklenicka V., Kardashev B.K., Kadomtsev A.G., Narykova M.V., Ivanov M.B. Elastic modulus, microplastic properties and durability of titanium alloys for biomedical applications. Rev. Adv. Mater. Sci. 2016. Vol. 45. No. 1/2. P. 42—51.</mixed-citation></citation-alternatives></ref><ref id="cit36"><label>36</label><citation-alternatives><mixed-citation xml:lang="ru">Кудряшов С.И., Голосова О.А., Колобова А.Ю., Колобов Ю.Р., Голосов Е.В. Сравнительное исследование особенностей наноструктурирования поверхностного рельефа αи β-титановых сплавов при импульсном фемтосекундном лазерном облучении // Композиты и наноструктуры. 2014. Т. 6. No. 3. С. 2—11.</mixed-citation><mixed-citation xml:lang="en">Kydryashov S.I., Golosova O.A., Kolobova A.Yu., Kolobov Yu.R., Golosov E.V. Sravnitel’noe issledovanie osobennostei nanostrukturirovaniya poverkhnostnogo rel’efa αi β-titanovykh splavov pri impul’snom femtosekundnom lazernom obluchenii [Comparative investigation of the features of the nanostructuring surface relief of αand β-titanium alloys at pulsed femtosecond laser irradiation]. Compozity i nanostructury. 2014. Vol. 6. No. 3. P. 2—11.</mixed-citation></citation-alternatives></ref><ref id="cit37"><label>37</label><citation-alternatives><mixed-citation xml:lang="ru">Колобов Ю.Р., Голосов Е.В., Раточка И.В. Особенности субмикрокристаллической структуры и ее влияние на механические свойства титановых сплавов // Вопр. материаловедения. 2008. T. 2 (54). С. 43—50.</mixed-citation><mixed-citation xml:lang="en">Kolobov Yu.R., Golosov E.V., Ratochka I.V. Osobennosti submikrokristallicheskoi struktury i eуe vliyanie na mekhanicheskie svoistva titanovykh splavov [Features of submicrocrystalline structure and its effect on mechanical properties of titanium alloys]. Voprosy materialovedeniya. 2008. Vol. 2 (54). P. 43—50.</mixed-citation></citation-alternatives></ref></ref-list><fn-group><fn fn-type="conflict"><p>The authors declare that there are no conflicts of interest present.</p></fn></fn-group></back></article>
